从催化裂化柴油中分离高纯度2,6-二甲基萘

以大庆石油化工总厂炼油厂催化柴油为原料 ,通过精馏分离得到二甲基萘 (DMN)窄馏分 (2 5 8～ 2 70℃ ) ,经糠醛溶剂抽提 ,减压蒸馏后 ,在 -10～ -2 5℃冷冻 2～ 5h ,离心分离制得纯度约 80 %的粗 2 ,6 DMN ,再经无水乙醇在 -10～ -2 5℃重结晶 ,得到纯度大于等于 98%的 2 ,6 DMN。     

丙烷脱沥青装置技术改造

对玉门炼油化工总厂 0 .2 5Mt/a丙烷脱沥青装置的技术改造情况进行了较为详细的介绍 ,对改造前后的操作参数、产品质量和经济技术指标进行了对比。改造后加工能力提高到 0 .30Mt/a ,装置的操作弹性大大提高 ,产品质量优良 ,溶剂单耗由 16 .1kg/t降至 1.6 7kg/t,能耗由 2 4 49.3MJ/t降至 1172 .3MJ/t,年经济效率达 30 0 0× 10 4RMB $。     

仙人掌绿色素的提取及稳定性研究

研究了墨西哥"米邦塔"仙人掌绿色素的提取工艺及光、热、微波、碳水化合物、常见的金属离子、有机酸和防腐剂等因素对仙人掌绿色素的影响,并研究了该色素的耐酸碱性、耐氧化性和耐还原性.结果表明:以无水乙醇为提取剂、料液比为2∶5、60℃条件下浸提40min,进行2次浸提效果最佳,且微波对浸提有一定的促进作用;该色素在中性和近中性溶液中相对稳定,有两个吸收峰分别在410nm和670nm处;对光、热、氧化剂敏感,对弱还原剂较稳定;在部分碳水化合物、有机酸、食盐、防腐剂溶液中不稳定;在金属离子中,除Na 、K 、Mg2 外,大多数金属离子对该色素无不良影响.     

稀疏脉冲反演技术在井间地震反演中的应用

将传统的波阻抗反演技术应用于井间地震资料反演时，存在着方法适用的域和资料的域不同，井间地震资料的频带比地震资料的频带宽以及频率比地震资料频率高，多对井间地震资料拼接等问题。为此，在胜利油田K71井区，探讨了利用传统波阻抗反演技术（稀疏脉冲反演）进行井间地震资料波阻抗反演的一些技术问题，并用利11对井间地震资料进行了波阻抗反演，获得了较好的反演结果，在井间地震资料反演中，采用匹配滤波方的井间地震资料转换到时间域；利用高分辨率地面三维地震资料，采用统计方法提取反演子波，子波的波形和相位较稳定，频带宽；对测井资料进行标准化处理，在反演的波阻抗剖面上砂体的空间展布形态清晰，对储层的描述更精细；利用时深转换模型，将时间域的波阻抗剖面转换到深度域，直接与测井资料进行对比分析，对储层的描述更直观可靠。     

Solids Extraction of Cod Frame and Effects on Ultrafiltration of the Aqueous Extract

Grinding, pH adjustment, heat treatment and centrifugation were studied to recover solids from ground cod frames and to apply ultrafiltration (UF) to the resulting aqueous phase. Early heat treatment (90°C/20 min) dissolved collagen into aqueous phase resulting in a very low UF flux. A pH adjustment to 4.5 after grinding (～0.32 cm die), with no heat resulted in efficient separation after centrifuging. UF of the aqueous phase showed an increase in initial flux (23 L/hr m²). However, when the same aqueous material was heated and then centrifuged (1–2% solids removed), UF flux was further increased to 46 L/hr m²and this process gave highest solids recovery (90%).     

Sunflower Head Residue Pectin Extraction as Affected by Physical Conditions

Effects of extraction pH, temperature, and time on yield and quality of pectin from sunflower heads (Interstate cultivar) were investigated. The low-methoxyl pectin was extracted, using 0.75% sodium hexametaphosphate at pH 3, 4, and 5 and at 75, 85, and 95°for 20, 40, and 60 min, respectively. Yield, molecular mass, and firmness of jellies of the pectins were determined. Three-way statistical analysis on yield, molecular mass and gel firmness showed strong interactions among pH, temperature and time. Highest yields were obtained at pH 5, 95°for 20 min and pH 4, 85°for 40 min. Pectin extracted for 40 min at pH 3 and 4 and at 85°and 75°C, respectively, had the highest molecular mass. Gel firmness of sunflower pectin prepared at pH 5.4 was higher than that of a commercial citrus pectin.     

膜萃取器设计及应用研究进展

简要阐述了膜萃取的特点和基本类型;重点介绍了轴对称、纤维、片状等３种膜器的设计原理、特征以及膜过程设计．总结了膜萃取技术在金属离子分离、旋光化合物的分离、发酵萃取、医药萃取等方面的应用现状和最新进展;展望了膜萃取技术的发展趋势。     

超临界CO2萃取技术及成套装备

介绍了超临界CO2 萃取这一新兴分离技术在工业化装置的工艺流程、化工过程、设备及过程控制系统等方面的内容     

Modeling of a power electronic converter for EMC in the conduction emission frequency band

With the advancement of high‐frequency switching devices, electromagnetic interferences (EMI) have become problems in power electronic converter designs. It is necessary for an electromagnetic compatibility (EMC) design to prospect and consider its possible EMI levels. This paper describes how to compute effects from a power converter to an object point to reduce conduction EMI noises effectively by an appropriate design. Modeling techniques for converter elements are discussed for a model in the conduction emission frequency band by the parameter tuning method and for line constants by an analytical derivation. Then a derived model is simulated for harmonic distributions of loop currents and their magnetic fields. © 2002 Scripta Technica, Electr Eng Jpn, 139(1): 44–50, 2002: DOI 10.1002/eej.1145     

Rapid analysis of polymer homologues and additives with SFE/SFC-MS coupling

A rapid and easy analysis method for polymers is presented. The method involves sample preparation by SFE, separation of the extracted compounds by SFC and simultaneous quantitative detection by FID, as well as identification of unknowns by MS. The applications illustrate how structural research work and routine polymer analysis can be done with this time saving method.